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Appearance:powder
Throughput:100|Kilogram|Month
pd_productuse:intermediate
Delivery Time:in stock
Purity:97% purity
Melting point 285°C(dec.)(lit.)
EPA Substance Registry System Aniline hydrobromide (542-11-0)
Safety Information
MSDS Information
ANILINE HYDROBROMIDE Usage And Synthesis
Purification Methods Crystallise the hydrobromide from water or EtOH and dry it at 5mm over P2O5. Also recrystallise it four times from MeOH containing a few drops of conc HBr by addition of pet ether (b 60-70o), then dry it to constant weight over paraffin chips in vacuo [Gutbezahl & Grunwald J Am Chem Soc 75 559 1953]. It precipitates from EtOH solution on addition of Et2O, and the filtered solid is recrystallised from EtOH and dried in vacuo. [Buchanan et al. J Am Chem Soc 108 1537 1986, Beilstein 12 III 232.]
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